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Electrophilic Aromatic Iodination of Vanillin
Essay specific features
Written by:
Holly L
Date added:
June 20, 2013
Level:
Grade:
A
No of pages / words:
4 / 874
Was viewed:
9154 times
Rating of current essay:
Essay content:
Used Purpose
3-methoxy-4-hydroxybenzaldehye C8H8O3 152.1494 MP=81-83, BP=285 NA 0.1g Solute
Ethanol CH3CH2OH 46.0688 MP=-114.1, BP=78.3 0.789 2.0mL Solvent
Sodium Iodide NaI 149.8943 MP=661, BP=1300 3.667 0.117g Catalyst
Bleach NaOCl 74.4422 MP=NA, BP=40dec 1.209 1.1mL Oxidizing Agent
Sodium Thiosulfate Na2O3S2 158...
displayed 300 characters
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Cool the flask in an ice bath for a few minutes. To the ice-cold solution, add 0.117 g of sodium iodide. Over a
period of 10 minutes, add 1.1 mL of Bleach (5.25% w/w NaOCl) dropwise to the cooled flask. The solution should turn a yellow color. Once the addition is complete, let the solution warm to room temperature and stir for about 10 minutes...
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