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Acetylation Of Ferrocene
Essay specific features
Written by:
Daniel Z
Date added:
July 28, 2013
Level:
University
Grade:
No of pages / words:
3 / 818
Was viewed:
4531 times
Rating of current essay:
Essay content:
The mixture was then refluxed with a calcium chloride drying tube for ten minutes and left to cool for an hour taking on a dark almost black colour. The reaction mixture was then poured onto ice (60 mL) and stirred to form brown mixture with some greenish black precipitate. Aqueous sodium hydroxide (37...
displayed 300 characters
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Aqueous sodium hydroxide (37.5 mL, 3M) was added to the mixture and solid sodium bicarbonate was added until the mixture was neutralised. The mixture was left to stand for an hour with stirring before the crude product was collected with vacuum filtration.The product was air dried for a couple of minutes then boiled with hexane (20 mL) leaving behind a brown- black gummy substance...
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