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Chapter 28: Nitration of Methyl Benzoate

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Issue:

Science

 

Written by:

Geneva V

 

Date added:

August 13, 2016

 

Level:

University

 

Grade:

A

 

No of pages / words:

2 / 465

 

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This is a highly exothermic reaction and is kept under control by means of cooling; after which the mixture is poured onto ice. The solid product will then be isolated by filtration and recrystallized from methanol, in which it is very soluable. A.) Materials: 1) .6mL of concentrated sulfuric acid 2) ...
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Data Collection Weights: Ice: 2.63g Crude Mass: .33g Refined Mass: .179g Methanol: 0.2mL Methyl Benzoate: .32g Melting Ranges: Crude Mass: 45-62 Celsius Refined Mass: 76-80 Celsius IV. Sample Calculations Ideal: Melting point of crude Methyl 3-nitrobenzoate of 74 – 76 degrees Celsius Melting point of refined Methyl 3-nitrobenzoate is 78 degrees Celsius Our: Crude Mass mp averages to 52...
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