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Chapter 28: Nitration of Methyl Benzoate
Essay specific features
Written by:
Geneva V
Date added:
August 13, 2016
Level:
University
Grade:
A
No of pages / words:
2 / 465
Was viewed:
2526 times
Rating of current essay:
Essay content:
This is a highly exothermic reaction and is kept under control by means of cooling; after which the mixture is poured onto ice. The solid product will then be isolated by filtration and recrystallized from methanol, in which it is very soluable.
A.) Materials:
1) .6mL of concentrated sulfuric acid
2) ...
displayed 300 characters
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Data Collection
Weights:
Ice: 2.63g
Crude Mass: .33g
Refined Mass: .179g
Methanol: 0.2mL
Methyl Benzoate: .32g
Melting Ranges:
Crude Mass: 45-62 Celsius
Refined Mass: 76-80 Celsius
IV. Sample Calculations
Ideal: Melting point of crude Methyl 3-nitrobenzoate of 74 – 76 degrees Celsius
Melting point of refined Methyl 3-nitrobenzoate is 78 degrees Celsius
Our: Crude Mass mp averages to 52...
displayed 300 characters
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