synthesis of dibenzalacetone

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Issue:

Science

 

Written by:

Rosa J

 

Date added:

December 19, 2012

 

Level:

University

 

Grade:

A

 

No of pages / words:

5 / 1324

 

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9727 times

 

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Essay content:

Used Mol. mp (K) bp (K) density(g/cm^3) acetone R11, R36, R67, S9, S25, S26 58.08 0.24 g 0.004 178.2 329.4 0.79 benzaldehyde R22, S24 106.13 0.82 g 0.008 247 451.1 1.0415 ehtyl acetate R11, R36, R66, R67, S16, S26, S33 88.11 2 ml per gram n/a 189.55 350.25 0.897 NaOH R35,S22, S26, S38, S45, S62, s24/25 39...
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The solution was then cooled to room temperature. Benzaldehyde (0.8ml; 9.82g, 0.008mol) was then added to the solution followed by addition of acetone (0.3ml; 0.24g, 0.004mol) and formed into a thick yellow solution. The flask was then swirled gently and constantly for 5 minutes. This turned into a fluffy precipitate as the flask was swirled...
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